A two-axis goniometer for low-temperature nuclear magnetic resonance measurements on single crystals.
- Shiroka T Laboratorium für Festkörperphysik, ETH Hönggerberg, CH-8093 Zürich, Switzerland. tshiroka@phys.ethz.ch
- Casola F
- Mesot J
- Bachmann W
- Ott HR
- 2012-10-02
Published in:
- The Review of scientific instruments. - 2012
English
We report on the construction of a two-axis goniometer intended for low-temperature, single-crystal nuclear magnetic resonance (NMR) measurements. With the use of home-made and commercially available parts, our simple probe-head design achieves good sensitivity, while maintaining a high angular precision and the ability to orient samples also when cooled to liquid helium temperatures. The probe with the goniometer is adapted to be inserted into a commercial (4)He-flow cryostat, which fits into a wide-bore superconducting solenoid magnet. Selected examples of NMR measurements illustrate the operation of the device.
- Language
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- English
- Open access status
- green
- Identifiers
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- DOI 10.1063/1.4748861
- PMID 23020388
- Persistent URL
- https://sonar.ch/global/documents/143386
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