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Monitoring polymer-assisted mechanochemical cocrystallisation through in situ X-ray powder diffraction.
Journal article

Monitoring polymer-assisted mechanochemical cocrystallisation through in situ X-ray powder diffraction.

  • Germann LS Max Planck Institute for Solid State Research, 70569 Stuttgart, Germany.
  • Emmerling ST Max Planck Institute for Solid State Research, 70569 Stuttgart, Germany.
  • Wilke M Laboratory for Synchrotron Radiation-Condensed Matter, Paul Scherrer Institute, Forschungsstrasse 111, 5232 Villigen PSI, Switzerland.
  • Dinnebier RE Max Planck Institute for Solid State Research, 70569 Stuttgart, Germany.
  • Moneghini M Department of Chemical and Pharmaceutical Sciences, University of Trieste, Piazzale Europa 1, 34127 Trieste, Italy. dhasa@units.it.
  • Hasa D Department of Chemical and Pharmaceutical Sciences, University of Trieste, Piazzale Europa 1, 34127 Trieste, Italy. dhasa@units.it.
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  • 2020-07-01
Published in:
  • Chemical communications (Cambridge, England). - 2020
Materials Chemistry
Electronic, Optical and Magnetic Materials
General Chemistry
Surfaces, Coatings and Films
Metals and Alloys
Ceramics and Composites
Catalysis
English Time-resolved mechanochemical cocrystallisation studies have so-far focused solely on neat and liquid-assisted grinding. Here, we report the investigation of polymer-assisted grinding reactions using in situ X-ray powder diffraction, revealing that reaction rate is almost double compared to neat grinding and independent of the molecular weight and amount of the polymer additive used.
Language
  • English
Open access status
closed
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Persistent URL
https://sonar.ch/global/documents/278557
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