A cryogen-consumption-free system for dynamic nuclear polarization at 9.4 T.
- Baudin M Laboratoire des biomolécules, LBM, Département de chimie, École normale supérieure, PSL University, Sorbonne Université, CNRS, 75005 Paris, France. Electronic address: mathieu.baudin@ens.fr.
- Vuichoud B Université de Lyon, CNRS, Université Claude Bernard Lyon 1, ENS de Lyon, Institut des Sciences Analytiques, UMR 5280, 69100 Villeurbanne, France.
- Bornet A Institut des sciences et ingénierie chimiques (ISIC), Ecole PolytechniqueFédérale de Lausanne (EPFL), 1015 Lausanne, Switzerland.
- Bodenhausen G Laboratoire des biomolécules, LBM, Département de chimie, École normale supérieure, PSL University, Sorbonne Université, CNRS, 75005 Paris, France.
- Jannin S Université de Lyon, CNRS, Université Claude Bernard Lyon 1, ENS de Lyon, Institut des Sciences Analytiques, UMR 5280, 69100 Villeurbanne, France.
- 2018-07-23
Published in:
- Journal of magnetic resonance (San Diego, Calif. : 1997). - 2018
Adiabatic cross polarization
Cryogen-consumption-free magnets
Dissolution DNP
Dynamic nuclear polarization (DNP)
English
A novel system for dissolution dynamic nuclear polarization based on a cost-effective "cryogen-free" magnet that can generate fields up to 9.4 T with a sample space that can reach temperatures below 1.4 K in a continuous and stable manner. Polarization levels up to P(1H) = 60 ± 5% can be reached with TEMPOL in about 20 min, and P(13C) = 50 ± 5% can be achieved using adiabatic cross polarization.
- Language
-
- English
- Open access status
- green
- Identifiers
-
- DOI 10.1016/j.jmr.2018.07.001
- PMID 30032035
- Persistent URL
- https://sonar.ch/global/documents/69777
Statistics
Document views: 10
File downloads:
- fulltext.pdf: 0